TA Instruments

AR1756-0008f

15/03/2013 15:07:30

Sample name	ASW Blank coupon#20 + DI + beads 275rad/s
Sample notes	 
Experiment notes	DI Deionised water, 25 mm diameter. 70 mm total depth of water, 10 mm gap, with PE beads
Operator	M Rides
Sample density	1.000 g/cm^3
Results file name	AR1756
Run number	8 
Results directory	D:\ARG2 rheometer\Test files\Southampton University P Stoodley May2012
Experiment was run on	15/03/2013 15:07:30

Procedure name	Flow procedure
Procedure notes	

Step name	Conditioning Step 1
Step notes	
Perform step	No
Initial temperature	20.0 C
Wait for correct temperature	Yes
Do set temperature	Yes
Wait for normal force	No
Perform pre-shear	No
Perform equilibration	Yes
Equilibration duration	0:00:30 hh:mm:ss
Wait for zero velocity	No
Control normal force	Uses current instrument settings
Purge gas only	No

Step name	Continuous ramp step 1
Step notes	
Perform step	No

Step name	Peak hold step
Step notes	
Perform step	Yes
Ramp type	Peak hold
Controlled variable	velocity 275.0 rad/s
Duration	0:01:00 hh:mm:ss
Delay time	0:00:01 hh:mm:ss
Temperature	20.0 C
Wait for temperature	No
Motor mode	auto 

Step name	Continuous ramp step 2
Step notes	
Perform step	No

Step name	Post-Experiment Step
Step notes	
Perform step	Yes
Do set temperature	Yes
Temperature	20.0 C
Set temperature system idle	No

Geometry name	25mm ETC plastic plate Southampton
Geometry notes	25 mm diameter parallel plastic plate with ETC rod
Geometry material	Other
Parallel plate diameter	25.00 mm
gap	10000 micro m
Gap offset	0 micro m
Geometry inertia	0.4094 micro N.m.s^2
Geometry compliance	2.020E-3 rad/N.m
Gap temperature compensation	0 micro m/C
Gap temperature compensation enabled	No
Shear rate factor	1.250 
Shear stress factor	3.259E5 1/m^3
Measurement system factor	2.608E5 1/m^3
Fluid density factor	1.278E-10 m^5
Normal force factor	4074 1/m^2
Backoff distance	5000 micro m
Approximate sample volume	4.91 ml

Sample compression	linear 
Compression distance	1000.0 micro m
Compression velocity	50.0 micro m/s
Fine velocity	500.0 micro m/s
Coarse velocity	6000.0 micro m/s
Other velocity	6000.0 micro m/s
Current temperature system	Peltier plate
Temperature control	Enabled 
Purge gas only	No
Temperature calibration	Peltier plate - 0.6 micro m/C
	Water bath - 0 micro m/C
	Torsion oven - plate - 0 micro m/C
	Torsion oven - solid sample - 0 micro m/C
	Peltier concentric cylinders - 0 micro m/C
	None - 0 micro m/C
	Stress relaxation - 0 micro m/C
	Current temperature system - 0 micro m/C
Cooling water temperature	15.0 C
Cooling water range	6.0 C
Bearing friction correction	Yes
Bearing friction	0.261 micro N.m/(rad/s)
Bearing offset	0 micro N.m
Temperature system span and offset	Peltier plate - span 1.0000 , offset 0 C
	Water bath - span 1.0000 , offset 0 C
	Torsion oven - plate - span 1.0000 , offset 0 C
	Torsion oven - solid sample - span 1.0000 , offset 0 C
	Peltier concentric cylinders - span 1.0000 , offset 0 C
	None - span 1.0000 , offset 0 C
	Stress relaxation - span 1.0000 , offset 0 C
	Current temperature system - span 1.0000 , offset 0 C
Bearing mapping type	precision 
Number of mapping iterations	2
Instrument type (MType)	AR-G2
Firmware version	  8.29  27/10/09
Configuration version (CnfVer)	301
Parameter version (PrmVer)	301
PCB Number	*NOT_SET*
IP address	192.168.1.2
Software version	V5.8.0
Windows version	Windows XP 5.1 (Service Pack 2)
Instrument inertia	21.14 micro N.m.s^2
Auto increment run number	Yes
Prompt for file name at start of run	Yes
Auto save results file	Yes
Results file storage	Consecutive steps of same type to 1 file 
Temperature tolerance	0.2 C
Temperature duration	0:00:10 hh:mm:ss
Wait for temperature even if OK	Yes
Gap tolerance	4 micro m
Gap duration	0:00:02 hh:mm:ss
Override wait for gap	No
Velocity tolerance	0.1000 rad/s
Zero speed after pre-shear	Leave as is 
Zero normal force before run	No
Zero timer before run	Before pre-shear 
Non-equilibrium minimum velocity	1.000E-4 rad/s
Zero strain at the start of each flow step	Yes
Inertia correction	Yes
Collect negative shear rate data if stress is positive	Yes
Collect all points	No
Display flow point graph during run	Yes
Store flow point graph with results	Yes
Store images to the results for flow steps	Yes
Creep zero displacement	Yes
Store images to the results for creep steps	Yes
Standard creep image store frequency	10 s
Repeated creep image store frequency in repeats	10 
Display oscillation waveform graph during run	Yes
Store oscillation waveform graph with results	Yes
Display strain control tries during run	Yes
Store strain control tries with results	Yes
Store images to the results for oscillation steps	Yes
Stress relaxation zero displacement	Yes
Store images to the results for stress relaxation steps	Yes
Flow torque limit	10.00 micro N.m
Flow velocity limit	1.000E-3 rad/s
Oscillation torque limit	5.00 micro N.m
Oscillation displacement limit	1.00E-5 rad
Oscillation raw phase limit	170.0 degrees
Oscillation minimum normal force limit	0.1000 N
Oscillation maximum normal force limit	50.00 N
Flow velocity tolerance	1.00 %
Oscillation torque tolerance	1.00 %
Oscillation displacement tolerance	1.00 %
Oscillation velocity tolerance	1.00 %
Temperature tolerance	1.0 C

Peak hold step

time	velocity	torque	gap	temperature	normal force	time global	shear stress	shear rate	viscosity	normal stress	displacement	normal stress coefficient	strain	% strain	1/temperature	time	time global
s	rad/s	micro N.m	micro m	C	N	s	Pa	1/s	Pa.s	Pa	rad	Pa.s^2			1/K	min	min

0.99200	274.7	-5274.6	10000	20.0	0.2238	0.992	-1719	343.4	-5.007	911.8	183.3870	7.734E-3	229.23	22923	3.411E-3	0.0	0.0
1.9920	275.0	589.99	10000	20.0	0.1897	1.992	192.3	343.7	0.5595	772.9	521.6190	6.543E-3	652.02	65202	3.411E-3	0.0	0.0
2.9920	275.0	584.19	10000	20.0	0.1852	2.992	190.4	343.7	0.5540	754.7	747.7700	6.389E-3	934.71	93471	3.411E-3	0.0	0.0
4.0040	275.0	579.97	10000	20.0	0.1254	4.004	189.0	343.7	0.5499	510.9	1086.9800	4.324E-3	1358.7	1.3587E5	3.411E-3	0.1	0.1
4.9920	275.0	580.04	10000	20.0	0.1721	4.992	189.1	343.7	0.5500	701.0	1313.0500	5.933E-3	1641.3	1.6413E5	3.411E-3	0.1	0.1
5.9920	275.0	561.13	10000	20.0	0.1787	5.992	182.9	343.7	0.5321	728.3	1539.3900	6.164E-3	1924.2	1.9242E5	3.411E-3	0.1	0.1
6.9920	275.0	560.72	10000	20.0	0.1852	6.992	182.8	343.8	0.5317	754.7	1878.8000	6.387E-3	2348.5	2.3485E5	3.411E-3	0.1	0.1
7.9920	275.0	566.94	10000	20.0	0.1861	7.992	184.8	343.7	0.5376	758.0	2104.8601	6.415E-3	2631.1	2.6311E5	3.411E-3	0.1	0.1
8.9960	275.0	546.66	10000	20.0	0.2045	8.996	178.2	343.8	0.5184	833.3	2444.0801	7.052E-3	3055.1	3.0551E5	3.411E-3	0.1	0.1
9.9920	275.0	551.78	10000	20.0	0.1479	9.992	179.9	343.8	0.5231	602.6	2670.3701	5.099E-3	3338.0	3.3380E5	3.411E-3	0.2	0.2
10.992	275.0	556.07	10000	20.0	0.2893	10.992	181.2	343.8	0.5272	1179	3009.4900	9.974E-3	3761.9	3.7619E5	3.411E-3	0.2	0.2
12.008	275.0	552.43	10000	20.0	0.1994	12.008	180.1	343.7	0.5238	812.6	3239.1101	6.877E-3	4048.9	4.0489E5	3.411E-3	0.2	0.2
12.992	275.0	558.81	10000	20.0	0.1775	12.992	182.1	343.8	0.5299	723.3	3471.9600	6.121E-3	4340.0	4.3400E5	3.411E-3	0.2	0.2
13.996	275.0	563.24	10000	20.0	0.1739	13.996	183.6	343.7	0.5341	708.4	3803.5901	5.997E-3	4754.5	4.7545E5	3.411E-3	0.2	0.2
14.992	275.0	548.94	10000	20.0	0.1781	14.992	178.9	343.7	0.5205	725.8	4027.4500	6.142E-3	5034.3	5.0343E5	3.411E-3	0.2	0.2
15.992	275.0	571.83	10000	20.0	0.1721	15.992	186.4	343.7	0.5422	701.0	4366.6299	5.933E-3	5458.3	5.4583E5	3.411E-3	0.3	0.3
16.992	275.0	556.87	10000	20.0	0.1787	16.992	181.5	343.7	0.5280	728.3	4593.0200	6.164E-3	5741.3	5.7413E5	3.411E-3	0.3	0.3
17.992	275.0	571.33	10000	20.0	0.1863	17.992	186.2	343.7	0.5418	758.9	4932.1499	6.423E-3	6165.2	6.1652E5	3.411E-3	0.3	0.3
18.996	275.0	564.50	10000	20.0	0.2023	18.996	184.0	343.7	0.5353	824.2	5158.5498	6.975E-3	6448.2	6.4482E5	3.411E-3	0.3	0.3
20.008	275.0	554.60	10000	20.0	0.3758	20.008	180.8	343.7	0.5259	1531	5500.2998	0.01296	6875.4	6.8754E5	3.412E-3	0.3	0.3
20.992	275.0	560.15	10000	20.0	0.2035	20.992	182.6	343.8	0.5311	829.1	5724.0098	7.016E-3	7155.0	7.1550E5	3.411E-3	0.3	0.3
21.992	275.0	544.71	10000	20.0	0.1787	21.992	177.5	343.8	0.5164	728.3	5950.1099	6.162E-3	7437.6	7.4376E5	3.411E-3	0.4	0.4
22.992	275.0	553.93	10000	20.0	0.1789	22.992	180.6	343.8	0.5252	729.1	6289.3999	6.170E-3	7861.8	7.8618E5	3.411E-3	0.4	0.4
23.996	275.0	567.54	10000	20.0	0.1787	23.996	185.0	343.7	0.5382	728.3	6517.7100	6.164E-3	8147.1	8.1471E5	3.411E-3	0.4	0.4
25.000	275.0	550.90	10000	20.0	0.1836	25.000	179.6	343.8	0.5223	748.1	6855.9902	6.330E-3	8570.0	8.5700E5	3.411E-3	0.4	0.4
26.008	275.0	555.24	10000	20.0	0.1812	26.008	181.0	343.7	0.5265	738.2	7081.1802	6.247E-3	8851.5	8.8515E5	3.411E-3	0.4	0.4
26.992	275.0	555.18	10000	20.0	0.1755	26.992	181.0	343.8	0.5264	715.1	7308.4800	6.051E-3	9135.6	9.1356E5	3.411E-3	0.4	0.4
27.996	275.0	550.73	10000	20.0	0.1826	27.996	179.5	343.8	0.5222	744.0	7646.5698	6.296E-3	9558.2	9.5582E5	3.411E-3	0.5	0.5
29.008	275.0	548.41	10000	20.0	0.1818	29.008	178.8	343.7	0.5200	740.7	7872.9399	6.269E-3	9841.2	9.8412E5	3.411E-3	0.5	0.5
30.008	275.0	554.77	10000	20.0	0.1781	30.008	180.8	343.8	0.5260	725.8	8214.0195	6.142E-3	10268	1.0268E6	3.411E-3	0.5	0.5
30.992	275.0	559.34	10000	20.0	0.1765	30.992	182.3	343.7	0.5304	719.2	8438.4102	6.087E-3	10548	1.0548E6	3.411E-3	0.5	0.5
31.992	275.0	552.99	10000	20.0	0.1771	31.992	180.2	343.7	0.5244	721.7	8777.4502	6.108E-3	10972	1.0972E6	3.411E-3	0.5	0.5
32.992	275.0	559.30	10000	20.0	0.1775	32.992	182.3	343.7	0.5303	723.3	9003.7598	6.121E-3	11255	1.1255E6	3.411E-3	0.5	0.5
33.988	275.0	559.81	10000	20.0	0.1737	33.988	182.5	343.7	0.5308	707.6	9345.2197	5.989E-3	11682	1.1682E6	3.411E-3	0.6	0.6
35.008	275.0	560.50	10000	20.0	0.1787	35.008	182.7	343.8	0.5315	728.3	9570.6104	6.163E-3	11963	1.1963E6	3.411E-3	0.6	0.6
35.992	275.0	551.67	10000	20.0	0.1775	35.992	179.8	343.7	0.5231	723.3	9796.3799	6.122E-3	12245	1.2245E6	3.411E-3	0.6	0.6
37.008	275.0	562.07	10000	20.0	0.1781	37.008	183.2	343.7	0.5330	725.8	10134.700	6.143E-3	12668	1.2668E6	3.411E-3	0.6	0.6
37.992	275.0	544.29	10000	20.0	0.1800	37.992	177.4	343.8	0.5161	733.2	10361.000	6.205E-3	12951	1.2951E6	3.411E-3	0.6	0.6
39.008	275.0	553.07	10000	20.0	0.1806	39.008	180.3	343.7	0.5245	735.7	10701.400	6.227E-3	13377	1.3377E6	3.411E-3	0.7	0.7
40.008	275.0	552.79	10000	20.0	0.1753	40.008	180.2	343.8	0.5242	714.2	10927.700	6.044E-3	13660	1.3660E6	3.411E-3	0.7	0.7
40.992	275.0	541.23	10000	20.0	0.1761	40.992	176.4	343.8	0.5132	717.5	11265.800	6.071E-3	14082	1.4082E6	3.411E-3	0.7	0.7
42.012	275.0	549.58	10000	20.0	0.1816	42.012	179.1	343.7	0.5211	739.9	11491.900	6.261E-3	14365	1.4365E6	3.411E-3	0.7	0.7
42.992	275.0	556.27	10000	20.0	0.1721	42.992	181.3	343.8	0.5274	701.0	11718.400	5.932E-3	14648	1.4648E6	3.411E-3	0.7	0.7
43.996	275.0	541.75	10000	20.0	0.1737	43.996	176.6	343.8	0.5136	707.6	12057.300	5.987E-3	15072	1.5072E6	3.411E-3	0.7	0.7
44.992	275.0	556.66	10000	20.0	0.1767	44.992	181.4	343.8	0.5278	720.0	12283.600	6.093E-3	15355	1.5355E6	3.411E-3	0.7	0.7
45.992	275.0	551.27	10000	20.0	0.1792	45.992	179.7	343.7	0.5228	729.9	12622.800	6.178E-3	15779	1.5779E6	3.411E-3	0.8	0.8
46.992	275.0	546.60	10000	20.0	0.1769	46.992	178.2	343.8	0.5183	720.8	12850.100	6.100E-3	16063	1.6063E6	3.411E-3	0.8	0.8
47.992	275.0	558.27	10000	20.0	0.1781	47.992	182.0	343.7	0.5294	725.8	13189.500	6.142E-3	16487	1.6487E6	3.411E-3	0.8	0.8
48.996	275.0	551.20	10000	20.0	0.1787	48.996	179.7	343.7	0.5227	728.3	13414.600	6.164E-3	16768	1.6768E6	3.411E-3	0.8	0.8
49.992	275.0	556.89	10000	20.0	0.1792	49.992	181.5	343.7	0.5281	729.9	13642.200	6.178E-3	17053	1.7053E6	3.411E-3	0.8	0.8
50.988	275.0	562.57	10000	20.0	0.1741	50.988	183.4	343.8	0.5334	709.3	13982.000	6.002E-3	17478	1.7478E6	3.411E-3	0.8	0.8
51.992	275.0	563.62	10000	20.0	0.1767	51.992	183.7	343.7	0.5345	720.0	14206.400	6.094E-3	17758	1.7758E6	3.411E-3	0.9	0.9
52.992	275.0	564.59	10000	20.0	0.1789	52.992	184.0	343.8	0.5353	729.1	14545.500	6.170E-3	18182	1.8182E6	3.411E-3	0.9	0.9
54.000	275.0	559.73	10000	20.0	0.1800	54.000	182.4	343.7	0.5308	733.2	14771.600	6.206E-3	18465	1.8465E6	3.411E-3	0.9	0.9
55.012	275.0	548.56	10000	20.0	0.1779	55.012	178.8	343.8	0.5201	725.0	15111.000	6.135E-3	18889	1.8889E6	3.411E-3	0.9	0.9
56.008	275.0	549.88	10000	20.0	0.1779	56.008	179.2	343.8	0.5213	725.0	15344.800	6.134E-3	19181	1.9181E6	3.411E-3	0.9	0.9
56.992	275.0	546.33	10000	20.0	0.1889	56.992	178.1	343.8	0.5180	769.6	15564.200	6.513E-3	19455	1.9455E6	3.411E-3	0.9	0.9
58.008	275.0	550.01	10000	20.0	0.1765	58.008	179.3	343.7	0.5215	719.2	15902.600	6.087E-3	19878	1.9878E6	3.411E-3	1.0	1.0
59.000	275.0	554.37	10000	20.0	0.1698	59.000	180.7	343.7	0.5257	691.9	16128.900	5.856E-3	20161	2.0161E6	3.411E-3	1.0	1.0
59.992	275.0	541.93	10000	20.0	0.1773	59.992	176.6	343.8	0.5139	722.5	16470.400	6.114E-3	20588	2.0588E6	3.411E-3	1.0	1.0

